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2 article(s) from Holmes, Andrew B

Controlled synthesis of poly(3-hexylthiophene) in continuous flow

Helga Seyler,
Jegadesan Subbiah,
David J. Jones,
Andrew B. Holmes and
Wallace W. H. Wong

Beilstein J. Org. Chem. 2013, 9, 1492–1500, doi:10.3762/bjoc.9.170

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Scheme 1: (a) Preparation of thiophene Grignard monomer and synthesis of P3HT by Kumada catalyst transfer pol...

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Figure 1: Plot of number-average molecular weight, M_n, versus monomer–catalyst ratio [M]₀/[I]₀ for batch and ...

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Figure 2: MALDI mass spectrum of low-molecular-weight preparation (GPC, M_n = 6.2 kg/mol) of P3HT in continuou...

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Figure 3: Plot of number-average molecular weight, M_n, versus monomer–catalyst ratio [M]₀/[I]₀ for batch and ...

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Scheme 2: Schematic representation of the telescoped preparation of P3HT in a flow reactor.

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Figure 4: ¹H NMR (CDCl₃, 500 MHz) spectra of P3HT samples prepared in (a) flow and (b) batch show comparable ...

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Figure 5: (a) Schematic diagram of the photovoltaic device geometry and (b) J–V curves of BHJ solar cells wit...

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Published 25 Jul 2013

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Enhancement of efficiency in organic photovoltaic devices containing self-complementary hydrogen-bonding domains

Rohan J. Kumar,
Jegadesan Subbiah and
Andrew B. Holmes

Beilstein J. Org. Chem. 2013, 9, 1102–1110, doi:10.3762/bjoc.9.122

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Figure 1: N-ethylhexyl-substituted (1) [20] and target free N–H (2) cyanopyridone structures.

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Scheme 1: Synthesis of the cyanopyridone 2, reagents and conditions: (i) Pd(PPh₃)₄, Cs₂CO₃, toluene, reflux, ...

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Figure 2: (a) Chloroform (solid line) and thin-film (dashed line) UV–vis absorption and emission spectra and ...

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Figure 3: The concentration dependence of (a) the NH ¹H NMR chemical shift and (b) the vinyl proton chemical ...

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Figure 4: AFM height image of observed nanostructures of films drop cast from (a) 10 mg/mL and (b) 1 mg/mL ch...

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Figure 5: Dimeric structures of 2. (a) centrosymmetric dimer of 2; (b) bond-rotated centrosymmetric dimer of 2...

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Figure 6: Schematic representation of self-complementary interactions leading to one-dimensional chains.

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Published 06 Jun 2013

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